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Two approaches have been used to anchor the heterometallic complex pwlladium the surface and generate monolayers. The first process consisted of depositing cluster 5 by spin coating on a gold surface.
The second was the immersion of a gold surface into a cluster solution. For both procedures, the resulting deposits were analysed by STM scanning tunneling microscopyellipsometry and XPS X-ray photoelectron spectroscopy. Xday the layers obtained by spin coating of a solution of cluster 5it was found that the cluster is not attached to the surface, but only deposited on it.
In contrast, after immersion of a gold substrate into a solution of 5 or 6anchoring of the complexes was clearly evidenced by XPS via the chemical shift of the S—2p binding energy toward lower binding energies. Ces couches ont ensuite été analysées par STM Scanning tunneling microscopypar ellipsométrie et par spectroscopie XPS X-ray photoelectron spectroscopy.
Mixed-metal clusters, Self-assembly, Gold surfaces, Spectroscopy, Scanning tunneling microscopy, X-ray photoelectron spectroscopy.
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Access to the PDF text. Access to the full text of this article requires a subscription. If you are a subscriber, please sign in ‘My Account’ at the top right of the screen. If you want to subscribe to this journal, see our rates You can purchase this item in Pay Palladuim View: Synthesis of functional heterometallic complexes and clusters containing molybdenum and palladium or platinum, their self-assembly on gold surfaces and X-ray photoelectron spectroscopic studies.
Outline Masquer le plan. Preparation of the xraay and analyses of the resulting layers. Top of the page – Article Outline.
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Experimental part Preparation of the gold substrates. Electronic supplementary information ESI available: CCDC reference numbers